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TECHNICAL PAPER




         2.6. Residual Properties of the concrete               2.6.6. Average optimum volume fraction of
         2.6.1. visual observations                             fibres
         The specimens were taken out of the furnace after 12 hours and   A relation with experimental data with error analysis, with
         observations were noted in terms of colour changes, cracking   respect to residual compressive strength and residual elastic
         patterns, crack widths, etc. to ascertain the degree of damages in   modulus has been developed to optimize percentage volume
         concrete specimens. In addition, the change in colour of basalt   fraction of basalt fibre in BFRC and in HyFRC (with 0.25% volume
         fibre was also studied for different elevated temperatures. The   fraction of PP fibres) exposed to different temperatures. The
         assessment in the colour change of PP fibres was not possible, as   validation of the formulation was carried out using experimental
         it melts at low temperature around 160ºC and evaporated. The   results.
         crack width formed in all specimens after temperatures exposure
         were measured with crack-width microscope.             Formulation
                                                                A function f 1 (x) is defined for a property varying with percentage
                                                                        120                               -200
                             o
                   Furnace Rate -6 C/min                        volume fraction (x) of the fibre for a particular exposure    30
                                                                        100
                                                                                                          -150
             1200  Specimen Rate -0.5°C/min       ASTM E-119-14  temperature t 1. The ‘z’ is a maximum value of percentage    25
                                                                        80ion for the property, i.e., in a sufficiently close
             1000                  Exposure       ISO 834-12    volume fract                              -100  Microvolt Endo Up (µV)  20
                                                                      Weight (%)
           Temperature ( o C)  800                Experimental - -  values of f 1 (x) is smaller than f 1 (x=z). The first derivative of the   Vee-Bee Time (seconds)  15
                                                                neighbourhood of the point, all values of ‘x’ are associated with
                                                                        60
                                                  Furnace
                                                                                                          -50
                                                                                                                              10
             600
                                                                        40
                                                  Experimental
                                                                                                             [49]
                                                                function is the extremum where the slope becomes zero  . In
                                                  Specimen
                                                                                                                              5
                                                                the present study, a quadratic equation for residual compressive
                                                                                                          0
             400
                                                                        20
             200                                                strength for various percentage volume fraction of fibre at a   0                Specimens Casted
                                                                         0
                                                                                                          50
                                                                given temperature based on the experimental results as given:
                                                                                                        1000
                                                                                200
                                                                                      400
                                                                          0
                                                                                                  800
                                                                                            600
               0
                0    200  400   600  800   1000                                      Temperature (˚C)  2                    Control  BFRC 1  BFRC 2  BFRC 3  HyFRC 1  HyFRC 2  HyFRC 3
                           Time (min)                                P  for a given temperature = f 1 (x) = ax  + bx + c  (1)
                                                                      1
                                                                                      TGA     DTA
            Figure 2: Surface temperature vs time for temperature exposure    where,
                                at 800ºC.
                                                                P 1  – Residual compressive strength (Property 1)
         2.6.2. Residual mass                                   x – Percentage volume fraction of fibres.
         Residual mass depicts the effect of exposure temperature on   At f’ 1                       [49]
             110
                                                                      60
         reduction in density of concrete. The percentage residual mass   to obtain the value of ‘x’, which yields an extremum of the   6                             Control
             100
           Residual Mass (%)
                                                                      50
         of the concrete specimens for each exposure temperature with   function f 1 (x). Similarly, the quadratic function for residual elastic   5                  BFRC 1
                                                                                                                                                                      BFRC 2
             90
                                                                      40
         respect to control specimens (25ºC) was calculated after 12   modulus is given below:                                                                        BFRC 3
             80
         hours of cooling.                                          Residual  Compressive Strength (MPa)(x) = 0, is a critical value of the argument  ; among them  (2)  Ultrasonic Pulse Velocity (km/s)  4 3  HyFRC 1
                                                                      30
                                                                    P  for a given temperature = f 1 (x) = Ax  + Bx + C
                                                                                                   2
                                                                     2
             70
                                                                                                                                                                      HyFRC 2
         2.6.3. Ultrasonic pulse velocity (UPv)                 where,  20                                                     2                                      HyFRC 3
             60
                                                                      10
             50
         The UPV was used to ascertain the degree of damages in terms   P 2  – Residual elastic modulus (Property 2).          1
                                                                       0
                                                        1200
                                           800
               0
                      200
                             400
                                    600
                                                 1000
         of quality of the concrete exposed to different temperatures.   0      200     400     600     800    1000
                                Temperature ( C)                x – Percentage volume fraction of fibres for the same          0
                                         o
                                                                                                 o
                                                                                        Temperature ( C)
         An UPV instrument of PUNDIT LAB PLUS of Proceq make with                                                                0     200   400    600    800   1000  1200
                 Control    BFRC 1      BFRC 2      BFRC 3      temperature at which the value of P  is obtained.  BFRC 3
                                                                                                 BFRC 2
                                                                          Control
                                                                                     BFRC 1
                                                                                            1
         transducers of 54 kHz frequency was used. The wave pattern of    HyFRC 1    HyFRC 2     HyFRC 3                                        Temperature ( C)
                                                                                                                                                        o
                                        HyFRC 3
                            HyFRC 2
                 HyFRC 1
         the concrete specimens exposed to different temperatures were   Similarly, at f’ 1 (x) = 0, is a critical value of the argument; among
         also recorded.                                         them to obtain the value of x, which yield an extremum of the
                                                                function f 1 (x).
         2.6.4 Residual compressive strength
                                                                A new function is defined as Y 1 (P 12, x) = f 1 (x) + f 1 (x) and its first
         Residual compressive strength of all the concrete specimens   derivative Y 1’ (P 12, x) is determined to seek the value of x, which
              40
         exposed to different temperatures were measured using UTM.   yield an extremum of the function for that particular temperature   0.8
                                                    Control
                                                                                        HyFRC
           Residual Elastic Modulus
              35
                                                    BFRC 1
                                                                         0.8
         The failure modes of each specimens were noted in order to   of study for the combined property. Experimental investigations   0.75          y = 6E-05x + 0.553
                                                                     Volume Fraction of Fibres
              30
                                                                         0.75
                                                                                                                               0.7
         assess the efficacy of fibres in concrete.  BFRC 2     was carried out with three different percentage volume fraction   0.65
                                                                                       y = 1E -05x + 0.5937
                                                    BFRC 3
              25
                                                                         0.7
                                                                                                             0.654
             (GPa)
                                                                       (PP+BF)%
                                                                         0.65
              20
                                                                                   0.607
                                                                              0.603
                                                    HyFRC 2
         2.6.5. Residual elastic modulus            HyFRC 1     of basalt fibre (0.5, 0.75 and 1%) for six different temperatures   Volume Fraction of Fibres (%)  0.6  0.57  0.559  0.566  0.573  0.604  0.62
                                                                         0.6
              15
                                                                                          0.587
                                                                and for two properties. In a similar way, the extremum point of
                                                                                    0.596
                                                    HyFRC 3
                                                                         0.55
                                                                                                      0.553
              10
         Elastic modulus were calculated for all the mixes exposed to   percentage volume fraction for all the six temperatures were   0.55
                                                                         0.5
                                                                                                                               0.5
               5
                                                                         0.45
         different temperatures by drawing a slope of the corresponding   determined for residual compressive and elastic modulus. A   0.45
               0
                                                                         0.4
                                 600
                                      800
                                            1000
                                                 1200
                           400
                0
         stress-strain curve at 40% of maximum stress of the specimens.  graph was plotted with extremum percentage volume fraction   0.4
                     200
                                                                                        400
                                                                                                                1200
                                                                                              600
                                                                                                    800
                                                                                                          1000
                                                                                 200
                                                                            0
                              Temperature ( C)                                            Temperature ( C)                       0      200   400    600    800    1000  1200
                                      o
                                                                                                   o
                                                                                                                                                          o
                                                                                                                                                 Temperature ( C)
                                                                            The IndIan ConCreTe Journal | auGuST 2019  19
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